Saturday, May 22, 2010

Determination Of Total Alkali As Na2O in Washing Soap

AIM:
To determine the total alkali as Na2O in the given sample of sunlight bar soap.
REAGENTS:
  • Methyl orange indicator
  • Distilled water: 30ml
  • N/2 Standard HCl

APPARATUS:

  • Conical flask
  • Water bath
  • Burette
  • Electronic balance

PROCEDURE:

  • Weigh accurately 10gm of the sliced soap sample using an electronic balance.
  • Note the weight taken.
  • Put the weighed sample into a clean conical flask.
  • Add 30ml distilled water.
  • Gently warm on a water bath to dissolve all the soap particle.
  • Cool for a while.
  • Titrate against N/2 std HCl from the burette using methyl orange as indicator.

CALCULATION:

Total alkali content as Na2O = (Volume of HCl * Normality of HCl *3.1)/weight of the sample.

RESULT:

I was able to calculate the total alkali content as Na2O in sunlight bar soap as 0.669 by taking 5gm of the sample.

Wednesday, March 3, 2010

About 'Alkali'

Any base or hydroxide eg: soda, potash etc that is soluble in water & can neutralise acids.Commonly used alkali's are Sodium hydroxide or caustic soda & Potassium hydroxide or caustic potash

Tuesday, March 2, 2010

What are Soaps?

Soaps are water soluble sodium or potassium salts of fatty acids. Soaps are made from fats & oils, or their fatty acids, by treating them chemically with a strong alkali.